Teflono TitanHeat
Heavy-duty PTFE grease with enhanced load capacity for 260-290°C environments
TitanHeat combines a perfluoropolyether (PFPE) base oil with a high-concentration PTFE dispersion for environments demanding both extreme temperature resistance and heavy load carrying capacity. The polyurea thickener eliminates metallic soap limitations, offering exceptional shear stability. Designed for steel mill bearings, cement kiln applications, and heavy industrial equipment operating at sustained high temperatures.
Temp Range
260°C — 290°C
PTFE Content
22%
Base Oil
PFPE (Perfluoropolyether)
NLGI Grade
2
Technical Data Sheet
Specifications
Additives
Key Features
- PFPE base oil for maximum thermal stability up to 290°C
- 22% PTFE content for heavy-load boundary lubrication
- Polyurea thickener eliminates metallic soap limitations
- MoS2 additive provides backup lubrication under extreme loads
- Exceptional shear stability for high-speed bearing applications
- Extended relubrication intervals reduce maintenance costs
Applications & Use Cases
Performance Characteristics
Manufacturing Recipe
Batch size: 1kg — Detailed formulation and step-by-step process
Ingredients (1kg batch)
| Ingredient | % | Grams | Role |
|---|---|---|---|
| PFPE Base Oil (Fomblin Y) | 45% | 450g | Base lubricant - fluorinated oil with extreme thermal stability |
| Polyurea Thickener | 12% | 120g | Non-soap thickener - superior thermal and shear stability |
| PTFE Micro-powder (3μm) | 22% | 220g | Solid lubricant - primary friction reducer and load bearer |
| Molybdenum Disulfide (MoS2) | 5% | 50g | Backup solid lubricant for extreme pressure conditions |
| MDI (Methylene Diphenyl Diisocyanate) | 6% | 60g | Polyurea precursor - reacts with amines to form thickener |
| Octadecylamine | 4% | 40g | Polyurea precursor - forms urea linkage with MDI |
| Phenolic Anti-oxidant (BHT) | 2% | 20g | Primary antioxidant - radical scavenger |
| Sulfurized EP Additive | 2.5% | 25g | Extreme pressure protection under shock loads |
| Benzotriazole Copper Passivator | 0.5% | 5g | Prevents copper corrosion in bronze bearings |
| Anti-foam Agent | 1% | 10g | Controls air entrainment |
Process Steps
PFPE Oil Heating
Heat PFPE base oil (Fomblin Y or equivalent) in a chemically inert vessel (PTFE-lined or glass). PFPE oils require careful handling - use only fluoropolymer-compatible seals and gaskets.
Polyurea Synthesis
Dissolve octadecylamine in half the PFPE oil at 70°C. Separately, dissolve MDI in the remaining PFPE oil at 50°C. Slowly combine the two solutions under vigorous agitation (1200 RPM). Exothermic reaction will occur - monitor temperature carefully.
Thermal Treatment
Heat the polyurea-PFPE mixture to drive the reaction to completion and develop the thickener structure. Maintain constant stirring. The mixture should develop a smooth, creamy consistency.
PTFE & MoS2 Incorporation
Cool to 140°C. Pre-blend PTFE micro-powder with MoS2 in a dry container. Add the dry blend slowly to the grease while agitating at 1500+ RPM. Continue mixing until fully homogeneous - approximately 15 passes through the high-shear zone.
Additive Addition
Cool to 110°C and add phenolic antioxidant, EP additive, copper passivator, and anti-foam agent. Mix each additive thoroughly for 5 minutes before adding the next.
Milling & Deaeration
Pass through a three-roll mill at tight clearances (0.02mm final gap) for ultra-smooth texture. Then deaerate under mild vacuum (500 mbar) for 15 minutes to remove trapped air.
Testing & Packaging
Perform full QC testing: penetration, drop point, EP testing, and oxidation stability. Package in steel containers with nitrogen blanket to prevent oxidation during storage.
Required Equipment
- PTFE-lined or glass-lined mixing vessel (2L)
- High-shear mixer (up to 1500+ RPM)
- Temperature controller with thermocouple
- Three-roll mill with adjustable gap
- Vacuum deaeration system
- Analytical balance (0.01g precision)
- Nitrogen gas supply for blanketing
- Full PPE: chemical-resistant gloves, respirator, face shield
Safety Notes
- MDI is a sensitizer and respiratory hazard - use in fume hood with appropriate respirator
- PFPE oils can decompose above 300°C releasing toxic fluorine compounds - do not overheat
- MoS2 dust is irritating - handle in well-ventilated area with dust mask
- Exothermic polyurea reaction requires careful temperature monitoring
- Keep water away from MDI - reacts violently with moisture
- Dispose of waste chemicals according to local hazardous waste regulations
Quality Control Checks
- Cone penetration: 265-295 dmm (ASTM D217)
- Drop point: >295°C (ASTM D2265)
- Four-ball wear scar: <0.40 mm (ASTM D2266)
- Four-ball EP weld point: >315 kgf (ASTM D2596)
- Oxidation stability: >300 min at 200°C (ASTM D942)
- Visual: Dark gray, smooth paste with no grit or separation
Where Competitors Still Lead
Full ComparisonTransparency matters — here are the specs where certain competitors outperform Teflono TitanHeat.